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tris(trimethylsilyl)silane

National Institutes of Health

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Silanes

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2017
2017
Amphiphilic acrylamide block copolymer: RAFT block copolymerization and monolayer behaviour
RAFT polymerization of acrylamide monomers with long alkyl sidechains was studied for application to block copolymer synthesis… 
2016
2016
Preparation of the Core Structure of Aspidosperma and Strychnos Alkaloids from Aryl Azides by a Cascade Radical Cyclization.
A novel approach to prepare the core structure of Aspidosperma and Strychnos alkaloids is described. The strategy is based on a… 
2009
2009
Thiomaleic anhydride: a convenient building block for the synthesis of alpha-substituted gamma- and delta-lactones through free-radical addition, nucleophilic ring opening, and subsequent…
Iodoalkyl tert-butyl carbonates and carbamates undergo clean free-radical addition to thiomaleic anhydride to give substituted… 
2008
2008
A new class of pyrazolopyridine nucleus with fluorescent properties, obtained through either a radical or a Pd arylation pathway from N-azinylpyridinium N-aminides.
The synthesis of dipyridopyrazole and pyridopyrazolopyrazine derivatives--both of which incorporate a 3-aryl moiety--can be… 
2006
2006
Synthesis of 2,4-disubstituted piperidines via radical cyclization: unexpected enhancement in diastereoselectivity with tris(trimethylsilyl)silane.
A novel approach to 2,4-disubstituted piperidines is reported, involving the radical cyclization of 7-substituted-6-aza-8… 
2001
2001
Reactivity of tris(trimethylsilyl)silane toward diarylaminyl radicals.
Absolute rate constants for the reaction of tri-tert-butylphenoxyl radical (ArO*) with (TMS)(3)SiH were measured… 
2000
2000
Synthesis of biaryls via intermolecular radical addition of heteroaryl and aryl bromides onto arenes
Tris(trimethylsilyl)silane (TTMSS) and azobisisobutironitrile (AIBN) promoted the easy intermolecular arylation of aryl and… 
2000
2000
Preparation of various C-2 branched carbohydrates using intramolecular radical reactions.
2000
2000
A Convenient Synthesis of 2′-Deoxy-2-fluoroadenosine; a Potential Prodrug for Suicide Gene Therapy
Abstract A convenient synthesis of 2′-deoxy-2-fluoro-adenosine (1) is described. Deaminative fluorination of 2-aminoadenosine (2… 
1997
1997
Photoreduction of Azoalkanes by Direct Hydrogen Abstraction from 1,4-Cyclohexadiene, Alcohols, Stannanes, and Silanes.
A mechanistic investigation of the photoreduction of the n,pi triplet-excited azo chromophore has been carried out on azoalkanes… 
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